Bragg diffraction

Bragg diffraction

Procedure

1. Arrange the setup like in the figure below:
   
2. Adjust the Transmitter and Receiver so that they directly face each other. Align the crystal so that the planes that you want to study are parallel to the incident microwave beam. Note that there are several sets of planes from which you can choose. Adjust the Receiver controls to provide a readable signal. Record the meter reading.
3. Rotate the crystal (with the rotating table) one degree clockwise and the Rotatable Goniometer arm two degrees clockwise. Record the grazing angle of the incident beam and the meter reading. (The grazing angle is the complement of the angle of incidence. It is measured with respect to the plane under investigation, not the face of the cube).
4. Continue in this manner, rotating the Goniometer arm two degrees for every one-degree rotation of the crystal. Record the angle and meter reading at each position.
5. Use your data, the known wavelength of the microwave radiation ($\lambda = 2.85\,\mathrm{cm}$), and Bragg’s Law to determine the spacing between the planes of the Bragg Crystal. Measure the spacing between the planes directly, and compare it with your experimental determination.

Results & analysis

The results of the measurement are shown in Figure 1 (below; note the error bars!).

We can identify clearly six peaks at $12^{\circ}$, $20^{\circ}$, $24^{\circ}$, $31^{\circ}$, $47^{\circ}$ and $59^{\circ}$. Considering that the wavelength of the source used to measure the diffraction is $\lambda=2.85\,\mathrm{cm}$, we use Bragg's law to obtain the following values for the interplane distance $d$:

Peak position ($^{\circ}$)	Diffraction order ($n$)	$d$
12	1	(6.12 $\pm$ 0.25)
20	1	(3.77 $\pm$ 0.09)
24	1	(3.17 $\pm$ 0.06)
31	1	(2.50 $\pm$ 0.03)
47	2	(3.53 $\pm$ 0.03)
59	2	(3.01 $\pm$ 0.02)

The actual separation between planes is $(3.80 \pm 0.05)\,\mathrm{cm}$, from which we can conclude that the peaks at 20$^{\circ}$ and at 47$^{\circ}$ correspond to the first and second diffraction orders of the planes. The other peaks, therefore, must be due to reflections with other planes of the crystal.

Useful links

• The data that I used for the analysis is here
• The manual to set up the experiment is here.